Contact

Eckhard Schleicher
Senior Scientist, Building Responsible Experimental Hall 771
Experimental Thermal Fluid Dynamics
e.schleicherAthzdr.de
Phone: +49 351 260 - 3230, 2103
Fax: +49 351 260 - 13230

Complex impedance needle probes

Objectives

For the investigation of multiphase and multi-component flows, which are of interest for instance in the chemical engineering or in oil extraction and processing, there are only few suitable measuring techniques. For this reason we have developed a high-speed complex impedance needle probe. Such probes are able to distinguish the different phases or components of a flow by measuring the complex value of the electrical impedance at a high data rate (up to 10,000 samples/s). The complex impedance probes can be applied, amongst others, for the investigation of:

  • oil-water-gas three-phase flows in the crude oil extraction and processing,
  • mixing of fluids, e.g. in chemical reactors,
  • fluid-gas two-phase flows.

Measuring principle

The measuring system consists of a needle probe in double coaxial geometry (see figure below) and proper electronic circuitry, responsible to generate and measure the signals involved in determining the complex impedance.

The determination of complex impedance is based on an amplitude and phase measurement of a sine wave signal at fixed frequency f (usually in the range of 200 kHz to 1 MHz). The complex impedance Zx can be obtained from the complex Ohm’s law

where Vin is the complex excitation voltage and Iout is the complex output current. A direct digital synthesizer generates the sine wave excitation voltage. The current in the measuring electrode is converted to a proportional voltage by means of a transimpedance amplifier. Both voltages signals (the excitation voltage and the amplifier output voltage) are then fed into an amplitude-phase detector, which determines the amplitude ratio and the phase difference of these signals. The developed probe electronics is able to determine the complex impedance at a frequency of 10 kHz.

Furthermore, the complex impedance Z measured by the probe is inversely proportional to the complex relative permitivitty εr* of the fluid under test according to

where ω denotes the angular frequency (ω = 2 π f), ε0 the permittivity of vacuum (8.85 pF/m), and kg the geometry factor of the probe.

Static measurements

The table below shows some measurements of the relative permittivity εr and conductivity σ carried out with the complex impedance needle probe for different liquids and air. The values in the table are the mean value of 20 measurements sampled at a frequency of 10 kHz. The excitation frequency was 200 kHz. The impedance needle probe was firstly calibrated on air and water, in order to measure the complex permittivity. Reference relative permittivity was taken from CRC Handbook of Chemistry and Physics. Reference conductivity was measured by a conductivity meter.

Substance
measured
εr
reference
εr
relative error [%]
measured
σ [µS/cm]
reference
σ [µS/cm]
relative error [%]
Air 1.05 1.00 5.00 -0.01 0.00 -
Glycol 41.22 40.56 1.62 1.44 1.50 4.00
2-propanol 20.52 19.74 3.95 0.097 0.10 3.00
Deionized water 79.17 79.86 0.86 2.58 2.50 3.20
Water + salt 81.92 79.86 2.57 32.24 33.20 2.89
Diethyl Ether 4.33 4.27 1.41 -0.02 0.0 -
Gasoline 2.02 2.0 - 2.3 ? -0.01 0.0 -
Silicone oil 2.61 2.58 1.16 -0.01 0.0 -

Three-phase flow measurement

The needle probe system has been employed to measure air and water bubbles flowing in gasoline (εr = 2.02). The excitation frequency was again 200 kHz and sampling frequency was 10 kHz per channel. The needle probe was located inside an acrylic glass column. The flow of bubbles was synchronously recorded with a high-speed video camera to evaluate the needle probe data.

First, air bubbles were generated at the bottom of the column. The following video shows the results for this experiment. The ascending air bubble is detected by the relative permittivity signal.

      click for video
       (AVI-video aprox. 5 MByte)

As a second experiment water bubbles with conductivity of 1.4 µS/cm were dropped into the column (see video below). The descending water bubble is sensed by both permittivity and conductivity signals.

      click for video
       (AVI-video aprox. 5 MByte)

Publications

Da Silva, M. J.; Schleicher, E.; Hampel, U.
A novel needle probe based on high-speed complex permittivity measurements for investigation of dynamic fluid flows
IEEE Transactions on Instrumentation and Measurement 56(2007)4, 1249-1256
doi:10.1109/TIM.2007.900419

Da Silva, M. J.; Brückner, F.; Schleicher, E.; Hampel, U.
High-speed complex admittance/permittivity needle probe for investigation of multiphase flows
23rd IEEE Instrumentation and Measurement Technology Conference, IEEE Instrumentation and Measurement Society, 24.-27.04.2006, Sorrento, Italy
Proceedings, 0-7803-9360-0, 1937-1941

Da Silva, M. J.; Hampel, U.; Schleicher, E.
Neue Konzepte für die kombinierte Leitfähigkeits- und Impedanzmessung in hochtransienten Mehrphasenströmungen
7. Dresdner Sensor-Symposium - Neue Herausforderungen und Anwendung in der Sensortechnik, 12.-14.12.2005, Dresden, Deutschland
Proceedings: TUDpress, 139-142


Contact

Eckhard Schleicher
Senior Scientist, Building Responsible Experimental Hall 771
Experimental Thermal Fluid Dynamics
e.schleicherAthzdr.de
Phone: +49 351 260 - 3230, 2103
Fax: +49 351 260 - 13230