Bachelor theses / Master theses / Diploma theses

X-ray fluorescence analysis (XRF) is a standard method to analyse a wide range of elements. Unfortunately, light elements (Z<11) are hard or impossible to analyse using XRF. On the other hand, LIBS (Laser induced breakdown spectroscopy) is able to analyse these elements. Especially the analysis of Lithium in solid samples is an urgent and currently needed topic. We aim to combine the two methods by developing an integrated workflow using fused beads, which is a standard technique for XRF sample preparation, for XRF analysis of the major elements and subsequent LIBS analysis for elements like e.g. Li.
Besides the development of a simple procedure to produce fused beads appropriate for both methods, calibration for both XRF and LIBS have to be implemented. The outcome of this (Master’s, Bachelor’s) thesis should be a as simple as possible workflow (including sample preparation), a sufficient number of reference materials (by e.g. mixing pure components), calibrations for XRF and LIBS, respectively and an evaluation of the desired method’s limitations. Motivated students of analytical chemistry, geosciences or adequate subjects are addressed.