Physical modelling of Czochralski crystal growth
Cz model experiments
At laboratory scales model experiments are an often used approach to industrial processes such as the Czochralski crystal growth method. Due to the availability of suitable measuring techniques, the low melting alloy GaInSn, which is liquid at room temperature became meanwhile as de facto standard.
The studies focus on the influence of various magnetic fields on the melt flow and the related heat transport in crucibles being heated from the bottom and/or side, and cooled by a crystal model covering about 1/3 of the upper melt surface.
Cz-model crucible | Experimental setup |
- Cz-model with a 7“ crucible perfectly fits to large-scale Si case
- independent rotation of crucible and crystal
Goal:
Electromagnetic control of melt flow, heat transfer and dopant distri-bution in electronic or photovoltaic silicon or GaAs, etc. growth processes
- Large scale buoyant flow in the crucible
- Temperature fluctuations and gradients at the interface crystal-melt-atmosphere
Methods:
- UDV flow measurements with small transducers (opaque fluids)
- Temperature measurements with fast and thin thermocouples
- Control by magnetic fields (MULTIMAG system)
Publications
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Grants, I.; Pal, J.; Gerbeth, G.
Physical modelling of Czochralski crystal growth in horizontal magnetic field
Journal of Crystal Growth 470(2017), 58-65 -
Poklad, A.; Pal, J.; Galindo, V.; Grants, I.; Heinze, V.; Meier, D.; Pätzold, O.; Stelter, M.; Gerbeth, G.
Magnetic flow control in growth and casting of photovoltaic silicon: Numerical and experimental results
IOP Conference Series: Materials Science and Engineering 228(2017)1, 012017 -
Wondrak, T.; Pal, J.; Stefani, F.; Galindo, V.; Eckert, S.
Visualization of the global flow structure in a modified Rayleigh-Bénard setup using contactless inductive flow tomography
Flow Measurement and Instrumentation (2017) -
Pal, J.; Cramer, A.; Grants, I.; Eckert, S.; Gerbeth, G.
Physical modelling of temperature fluctuations in a high aspect ratio model of the Czochralski crystal growth
Journal of Crystal Growth 432(2015), 69-77 -
Pal, J.; Cramer, A.; Gerbeth, G.
Experimental investigation on the electromagnetically controlled buoyancy-induced flow in a model of a Czochralski puller
International Journal of Applied Electromagnetics and Mechanics 44(2014), 163-170 -
Cramer, A.; Pal, J.; Gerbeth, G.
Ultrasonic flow measurements in a model of a Czochralski puller
Flow Measurement and Instrumentation 37(2014), 99-106 -
Cramer, A.; Pal, J.; Gerbeth, G.
Model experiments for the Czochralski crystal growth technique
European Physical Journal - Special Topics 220(2013), 259-273