Contact

Johanna Sohr
Experimental Thermal Fluid Dynamics
j.sohrAthzdr.de
Phone: +49 351 260 - 3197

Dr. Markus Schubert
Experimental Thermal Fluid Dynamics
m.schubertAthzdr.de
Phone: +49 351 260 - 2627
Fax: +49 351 260 - 2383

Experimental and theoretical investigations of fluid dynamics and mass transfer in sandwich packings

Sub-project: Characterization of fluid dynamics using ultrafast X-ray tomography

Similar to random or conventional structured packings, sandwich packings are employed to promote large contact between gaseous and liquid phases in separation columns operated in a counter-current mode. Such sandwich packings consist of two corrugated sheet layers with different specific surface area, arranged alternately inside the column. As a result, bubbly flow evolves in the hold-up layer. Compared to conventional packed columns, the interaction between the involved phases is strongly intensified, in particular in the bubbly flow area and the evolving froth regime. This leads to higher separation efficiency of the column, further accompanied by reduced energy consumption.



Within the scope of the DFG-funded project, the fluid dynamic behavior of sandwich packings is comprehensively studied at HZDR. For this purpose, experimental studies are carried out in a 100 mm diameter column operated with water and air in the counter-current mode. The ultrafast X-ray tomography permits noninvasive imaging of the complex and highly dynamic flow patterns inside the packing. Crucial parameters such as liquid holdup, gas-liquid interfacial area and froth height are determined. Furthermore, pressure sensors precisely measure the axial pressure gradient along the column height, thereby revealing information about the transitions zones between the evolving flow configurations.

The gathered data of the fluid dynamics will be correlated and implemented in a modelling approach to provide tools for the design of columns with sandwich packings and for the prediction of their separation efficiency.



Cooperation

  • Paderborn University, Chair of Fluid Process Engineering

Funding

Deutsche Forschungsgemeinschaft (DFG, HA3088/10-1)

References

  • M. Schubert, A. Bieberle, F. Barthel, S. Boden, U. Hampel (2011)
    Advanced tomographic techniques for flow imaging in columns with flow distribution packings.
    Chemie Ingenieur Technik 83, 7, 979-991.
  • A. Janzen, M. Schubert, F. Barthel, U. Hampel, E. Y. Kenig (2013)
    Investigation of dynamic liquid distribution and hold-up in structured packings using ultrafast electron beam X-ray tomography
    Chemical Engineering and Processing 66, 20-26.
  • S. Flechsig, Ö. Yildirim, E. Y. Kenig (2016)
    Sandwich Packings: State of the Art
    ChemBioEng Reviews 3, 174-185.
  • J. Sohr, A. Litzka, M. Schubert, S. Flechsig, E. Y. Kenig, U. Hampel (2017)
    Untersuchung heterogener Strömungsmuster in Anstaupackungen mittels ultraschneller Röntgentomographie: Methode und Validierung
    Jahrestreffen der ProcessNet Fachgruppe Fluidverfahrenstechnik, 8-10. März 2017, Köln.
  • S. Flechsig, J. Sohr, M. Schubert, U. Hampel, E. Y. Kenig (2017)
    Anwendung von Anstaupackungen bei der CO2-Absorption in wässrigen Aminlösungen
    Jahrestreffen der ProcessNet Fachgruppe Fluidverfahrenstechnik, 8-10. März 2017, Köln.


Contact

Johanna Sohr
Experimental Thermal Fluid Dynamics
j.sohrAthzdr.de
Phone: +49 351 260 - 3197

Dr. Markus Schubert
Experimental Thermal Fluid Dynamics
m.schubertAthzdr.de
Phone: +49 351 260 - 2627
Fax: +49 351 260 - 2383