Single-crystal X-ray diffraction and resonant X-ray magnetic scattering at helium-3 temperatures in high magnetic fields at beamline P09 at PETRA III
Single-crystal X-ray diffraction and resonant X-ray magnetic scattering at helium-3 temperatures in high magnetic fields at beamline P09 at PETRA III
Francoual, S.; Strempfer, J.; Warren, J.; Liu, Y.; Skaugen, A.; Poli, S.; Blume, J.; Wolff-Fabris, F.; Canfield, P. C.; Lograsso, T.
The resonant scattering and diffraction beamline P09 at PETRA III at DESY is equipped with a 14 T vertical field split-pair magnet. A helium-3 refrigerator is available that can be fitted inside the magnet's variable-temperature insert. Here the results of a series of experiments aimed at determining the beam conditions permitting operations with the He-3 insert are presented. By measuring the tetragonal-to-orthorhombic phase transition occurring at 2.1 K in the Jahn-Teller compound TmVO4, it is found that the photon flux at P09 must be attenuated down to 1.5 x 109 photons s-1 for the sample to remain at temperatures below 800 mK. Despite such a reduction of the incident flux and the subsequent use of a Cu(111) analyzer, the resonant X-ray magnetic scattering signal at the Tm LIII absorption edge associated with the spin-density wave in TmNi2B2C below 1.5 K is intense enough to permit a complete study in magnetic field and at sub-Kelvin temperatures to be carried out.
Involved research facilities
- High Magnetic Field Laboratory (HLD)
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Journal of Synchrotron Radiation 22(2015), 1207-1214
DOI: 10.1107/S1600577515014149
ISSN: 1600-5775
Cited 3 times in Scopus
Permalink: https://www.hzdr.de/publications/Publ-22404